Structural, electrical and magnetic studies on CoFe2O4 nanoparticles with polyvinylalcohol (PVA) via Sol-Gel approach

被引:0
|
作者
Lakshmigandhan, T. [1 ]
Nithiyanantham, S. [1 ]
Mahalakshmi, S. [2 ]
Kogulakrishnan, K. [1 ]
Mohan, R. [3 ]
Gunasekaran, B. [4 ]
Palaniappan, L. [5 ]
机构
[1] Bharathidasan Univ Thiruchirapalli, Thiru Vi Ka Govt Arts Coll, Nanomagnet & Femtosci Div, Dept Phys, Thiruchirapalli 610003, India
[2] Ethiraj Coll Women Chennai, Dept Phys, Chennai 600008, Tamilnadu, India
[3] AMET Univ, Dept Chem, Chennai 603112, Tamilnadu, India
[4] SRM Inst Sci & Technol, Dept Phys & Nanotechnol, Chennai 603203, Tamilnadu, India
[5] Annamalai Univ, Dept Phys, Annamalainagar 602008, Tamilnadu, India
关键词
Sol; -gel; Cobalt ferrite; PVA; magnetic property; Nanopartaicle; dielectric property; electrochemical; COBALT FERRITE NANOPARTICLES; PHASE EVOLUTION; DRUG-DELIVERY; HYPERTHERMIA; TEMPERATURE; COMBUSTION; SIZE; PH;
D O I
10.1016/j.mseb.2024.117494
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
Cobalt ferrite (CoFe 2 O 4 ) nanoparticles were synthesized using sol-gel method from cobalt nitrate; iron nitrate as precursor materials with the chelating agent PVA in water (2.5, 5.0, 7.5, 10.0 and 12.5 %) is added. Through Xray diffraction (XRD) examinations, the crystallite size and single phase of the ferrite samples were studied. The functional and active analysis is found through Fourier transform infrared (FTIR) studies. The optical analysis carried out through UV-visible spectrometer and the absorption is found. The surface features and its content of elements were analyzed through SEM with EDAX analysis. The larger saturation magnetization at 12.5 % were recorded through vibrating sample magnetometer (VSM). The dielectric behavior recorded at room temperature from LCR measurement. The electrochemical behavior like V/I, impedance, scan rate and phase angle obtained through cyclic voltameter setup. The observed results with all the physical parameters with the influence of presence of PVA are discussed and interpreted extensively.
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页数:10
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