Dynamic process of wet etching using BOE solutions to control the etch rate, roughness, and surface morphology of a Z-cut α-quartz wafer

被引:2
|
作者
Xue, Hong [1 ,2 ]
Zhang, Zichao [1 ,2 ]
Ai, Jiabin [1 ,2 ]
Li, Cun [1 ,2 ]
Li, Bo [1 ,2 ]
Zhao, Yulong [1 ,2 ]
Wang, Aihua [2 ,3 ]
机构
[1] Xi An Jiao Tong Univ, State Key Lab Mfg Syst Engn, Xian 710049, Shaanxi, Peoples R China
[2] Xi An Jiao Tong Univ, Sch Mech Engn, Xian 710049, Peoples R China
[3] Shaanxi Inst Metrol Sci, Xian 710100, Shaanxi, Peoples R China
基金
中国国家自然科学基金;
关键词
MEMS; Wet etching; Quartz; Roughness; Morphology; PRESSURE SENSORS; ARRAY; FABRICATION;
D O I
10.1016/j.ceramint.2024.04.340
中图分类号
TQ174 [陶瓷工业]; TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
Quartz is a widely used material in the field of microelectromechanical systems (MEMS) for fabricating devices such as substrates, probes, and lenses; it is also indispensable as a resonator or oscillator for frequency control in communication and network technologies. However, its development is limited because it is difficult to fabricate an ideal profile for implementation in complex structures. In practice, wet etching is the most effective and extensive method for achieving the expected structure, although dry etching and other special machining techniques have also been investigated. In this study, the dynamic wet etching process was recorded using different ratios of buffered oxide etcher (BOE) solutions as the etchant to reveal the etching mechanism. The experiments were first designed considering the fabrication of samples, experimental conditions, and measurement indicators. Subsequently, the corresponding etch rate, roughness, and surface morphology were investigated to control the process parameters during wet etching. Different etchants exhibit varying etching rates and roughness properties. A smaller proportion of hydrofluoric acid in the BOE solution results in lower etch rate, and vice versa. The roughness (Ra) in the stable stage was not completely consistent with the tendency of the etch rate, whereas the surface morphology and dimensions of the pyramids rationally complied with the roughness trend. Additionally, the results suggested that the three following stages exist during the wet etching process of the z-cut alpha-quartz wafer; smooth, incremental, and stable. The analysis of the dynamic wet etching process in this study is beneficial for the structural design, manufacturing, and performance of quartz MEMS devices.
引用
收藏
页码:25978 / 25987
页数:10
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