Magnetic Solid-Phase Extraction with Dispersion of Magnetic Hypercrosslinked Polystyrene by Carbon Dioxide for the Extraction of Amphenicols from Honey and Milk in Their Determination by HPLC-MS/MS

被引：0
|
作者：
Goncharov, N. O. [1 ]
Tolmacheva, V. V. [1 ]
Lazarevich, T. V. [1 ,2 ]
Melekhin, A. O. [3 ]
Puryskin, I. D. [1 ]
Apyari, V. V. [1 ]
Dmitrienko, S. G. [1 ]
机构：
[1] Lomonosov Moscow State Univ, Dept Chem, Moscow 119991, Russia
[2] Univ Leipzig, D-04109 Leipzig, Germany
[3] Fed Ctr Anim Hlth, Vladimir 600901, Russia
来源：
JOURNAL OF ANALYTICAL CHEMISTRY | 2024年 / 79卷 / 09期
关键词：
amphenicols; honey; milk; magnetic solid-phase extraction; effervescent extraction; magnetic hypercrosslinked polystyrene; HPLC-MS/MS; POLYCYCLIC AROMATIC-HYDROCARBONS; EFFERVESCENT TABLETS; IONIC LIQUIDS; ORGANIC FRAMEWORKS; MICROEXTRACTION;
D O I：
10.1134/S1061934824700655
中图分类号：
O65 [分析化学];
学科分类号：
070302 ; 081704 ;
摘要：
A magnetic solid-phase extraction method with the dispersion of magnetic hypercrosslinked polystyrene (MHCPS) by carbon dioxide is proposed for the extraction and preconcentration of amphenicols (chloramphenicol, florfenicol, and thiamphenicol) from honey and milk before their determination by HPLC-MS/MS. Effervescent tablets, consisting of sodium bicarbonate, citric acid, and MHCPS in the case of honey and sodium bicarbonate and MHCPS in the case of milk, were used. The conditions for obtaining tablets were selected (the amount and ratio of the acid, base, and MHCPS in the composition of a tablet and its mass), ensuring the quantitative release of amphenicols. Procedures for the determination of amphenicols in honey and milk with the dispersion of the sorbent by carbon dioxide and the subsequent determination of the compounds by HPLC-MS/MS are developed. The limits of detection are 0.3-1 and 0.02-0.05 mu g/kg for honey and milk, respectively.
引用
收藏
页码：1296 / 1303
页数：8
相关论文
共 50 条
  • [1] Determination of Chloramphenicol in Honey with Automated Solid-Phase Extraction and HPLC-MS/MS Detection
    Wollseifen, Hans Rainer
    Brand, Johannes
    Lambrecht, Detlef
    [J]. LC GC EUROPE, 2017, 30 (12) : 694 - 695
  • [2] Determination of octreotide in human serum by HPLC-MS/MS with solid-phase extraction
    Capron, A.
    Destree, J.
    Wallemacq, P.
    [J]. THERAPEUTIC DRUG MONITORING, 2011, 33 (04) : 559 - 559
  • [3] Magnetic dispersive solid-phase extraction based on a novel adsorbent for the detection of triazole pesticide residues in honey by HPLC-MS/MS
    Miao, Qiongchen
    Wang, Jianmei
    Nie, Jing
    Wu, Huizhen
    Liu, Yanping
    Li, Zuguang
    Qian, Mingrong
    [J]. ANALYTICAL METHODS, 2016, 8 (26) : 5296 - 5303
  • [4] Determination of Midazolam in Animal Tissues by Solid-Phase Extraction HPLC-MS/MS Method
    Zhao, Jianyuan
    Zhao, Yan
    Yang, Shuming
    Zhang, Bin
    Wei, Tao
    [J]. ASIAN JOURNAL OF CHEMISTRY, 2014, 26 (16) : 5235 - 5238
  • [5] Facile synthesis of magnetic hypercrosslinked polystyrene and its application in the magnetic solid-phase extraction of sulfonamides from water and milk samples before their HPLC determination
    Tolmacheva, Veronika V.
    Apyari, Vladimir V.
    Furletov, Aleksei A.
    Dmitrienko, Stanislava G.
    Zolotov, Yury A.
    [J]. TALANTA, 2016, 152 : 203 - 210
  • [6] Determination of pyrrolizidine alkaloids in honey from selected sites by solid phase extraction and HPLC-MS
    Crews, C
    Startin, JR
    Clarke, PA
    [J]. FOOD ADDITIVES AND CONTAMINANTS, 1997, 14 (05): : 419 - 428
  • [7] Rapid Determination of Trace Sulfonamides in Milk by Graphene Oxide-Based Magnetic Solid Phase Extraction Coupled with HPLC-MS/MS
    Wang, Yutang
    Liu, Laping
    Xiao, Chunxia
    Chen, Lin
    Yang, Peng
    Liu, Qian
    Wang, Jianlong
    Liu, Xuebo
    [J]. FOOD ANALYTICAL METHODS, 2016, 9 (09) : 2521 - 2530
  • [8] Molecularly imprinted solid phase extraction method for simultaneous determination of seven nitroimidazoles from honey by HPLC-MS/MS
    Guo, Xiu-Chun
    Xia, Zhao-Yang
    Wang, Hai-Hui
    Kang, Wen-Yi
    Lin, Li-Ming
    Cao, Wen-Qing
    Zhang, Hong-Wei
    Zhou, Wen-Hui
    [J]. TALANTA, 2017, 166 : 101 - 108
  • [9] Magnetic Solid-Phase Extraction Based on Magnetic Sulfonated Reduced Graphene Oxide for HPLC-MS/MS Analysis of Illegal Basic Dyes in Foods
    Cui, Shibo
    Mao, Xinwu
    Zhang, Haijing
    Zeng, Haowei
    Lin, Zihao
    Zhang, Xuewu
    Qi, Ping
    [J]. MOLECULES, 2021, 26 (24):
  • [10] Surface molecularly imprinted solid-phase extraction for the determination of vancomycin in plasma samples using HPLC-MS/MS
    Zhou, Hao
    Chen, Qianqian
    Song, Xuqin
    He, Limin
    Liu, Rong
    [J]. ANALYTICAL SCIENCES, 2022, 38 (09) : 1171 - 1179
12345