Extraction of Volatile Compounds and Analysis of Aroma Characteristics in Fenggang Zinc-Selenium Tea

被引:0
|
作者
He T. [1 ]
Wu Q. [1 ]
Xiang L. [2 ]
Feng H. [1 ,2 ]
机构
[1] School of Pharmacy, Zunyi Medical University, Zunyi
[2] Institute of Producst Quality Inspection & Testing of Zunyi City, Zunyi
关键词
extraction process; Fenggang zinc-selenium tea; gas chromatography-mass spectrometry; headspace solid-phase microextraction; orthogonal partial least squares discriminant analysis; principal component analysis;
D O I
10.13386/j.issn1002-0306.2022100238
中图分类号
学科分类号
摘要
In order to explore the variation of volatile components of Fenggang zinc-selenium tea during the production process. The combination of headspace solid phase microextraction (HS-SPME) with gas chromatography-mass spectrometry (GC-MS) was applied to detecte volatile components of Fenggang zinc-selenium tea during the production process, and optimize the extracting conditions. Principal component analysis and orthogonal partial least squares discriminant analysis were used to determine, distinguish and screen the volatile components of Fenggang zinc-selenium tea during the production process. The results showed that the best extraction process was as follows: Ratio of raw material to water was 1:6 (g/mL), extraction fiber 50/30 μm CAR/DVB/PDMS, extraction temperature at 90 ℃, extraction time for 70 min. A total of 91 volatile substances were identified by GC-MS that there were 37 kinds of common characteristic volatile components in the Fenggang zinc-selenium tea during the production process. Alcohols, ketones, esters and aldehydes were the main volatile components constituting the aroma of Fenggang zinc-selenium tea, among which alcohols were the most abundant and the highest content. Fenggang zinc-selenium tea could be divided into one category before processing and one category after processing by principal component analysis, and orthogonal partial least squares discriminant analysis showed that 15 volatile components contributed significantly to the odor of Fenggang zinc-selenium tea. Jasmonone, (S)-oxidized linalool, α-ionone, methyl salicylate, methyl heptenone, (E)-oxidized linalool, cedarol, βcyclic citral, 2-pyrrol 6-trimethyl-6-vinyl tetrahydro-2H-furan-3-ol and methyl acetylsalicylate played an important role in the characteristic aroma quality of Fenggang zinc-selenium tea. This study can provide a theoretical basis for the production, processing, quality control of Fenggang zinc-selenium tea. © 2023 Editorial Department of Science and Technology of Food Science. All rights reserved.
引用
收藏
页码:342 / 351
页数:9
相关论文
共 32 条
  • [1] ZHANG P Y, LI R, LI H Y, Et al., Analysis of voltatile compounds in Chrsanthemum moriflium Ramat by HS-SPME-GC MS/MS combing retenyion index[J], Food and Fermentation Industries, 45, 1, pp. 202-209, (2019)
  • [2] XU F, LI E Y, CHU Z, Et al., Optimization of flavor components of Vanilla concentrate by headspace solid phase microextraction-GC mass spectrometry analysis[J], Chinese Journal of Tropical Crops, 40, 2, pp. 348-358, (2019)
  • [3] YU J, YANG J, LI M, Et al., Protective effects of Chinese Fenggang zinc selenium tea on metabolic syndrome in high-sucrose-high-fat diet-induced obese rats[J], Scientific Report, 8, 1, (2018)
  • [4] WANG X N, ZHAO R R, ZHANG J Y., Global metabolic regulation of Fenggang zinc-selenium tea in normal rat based on metabolomics technology[J], Science and Technology of Food Industry, 41, 6, (2020)
  • [5] LUO D L, SHAO Y, BA L J, Et al., Electronic nose identification and analysis of aroma components of four famous and excellent teas in Guizhou[J], Storage and Process, 20, 3, pp. 183-190, (2020)
  • [6] YANG C, YAN H F, LU X Y, Et al., Geographical origin discrimination of Anhua dark tea by elemental fingerprint[J], Food Science, 41, 16, pp. 286-291, (2020)
  • [7] LIN J Z, TU Z, CHEN L, Et al., The effect of red light withering on the volatile components of leaves and quality of blank tea product[J], Journal of Tea Science, 41, 3, pp. 393-405, (2021)
  • [8] JIANG B, YAN Y Z, LIU K Y, Et al., Comparison of the difference between Yunnan and Fujian white tea[J], Journal of Southwest University (Natural Science Edition), 43, 4, pp. 62-72, (2021)
  • [9] LI Y D, HUANG Y, LIU X Y, Et al., Comparative analysis of volatile components in fu brick tea by simultaneous distillation and headspace solid-phase micro-extraction [J], Science and Technology of Food Industry, 39, 24, pp. 246-252, (2018)
  • [10] ERDEM P, TAGAC A A, BOZKURT S S, Et al., Chitosan and dicationic ionic liquid intercalated clay-coated solid-phase microextraction fiber for determination of sixteen polycyclic aromatic hydrocarbons in coffee and tea samples[J], Talanta, 235, (2021)