Synthesis and Crystal Structure of Tert-butyl 4-[(E)-4-(1,3-Dioxo-1,3-dihydro-2H-isoindol-2-yl)-1-butenyl] Benzoate

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作者：
张新歌
张慧杰
王瑱
李朝兴
机构：
[1] InstituteofPolymerChemistry,NankaiUniversity
来源：
结构化学. | 2006年 / 03期
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摘要：
The title compound tert-butyl 4-[(E)-4-(1,3-dioxo-1,3-dihydro-2H-isoindol-2-yl)- 1-butenyl] benzoate has been synthesized and characterized by X-ray crystallography. It crystallizes in monoclinic, space group C2/c with a = 14.875(3), b = 8.9796(13), c = 34.736(6) ?, β = 95.981(4)o, V = 4614.4(14) ?3, Z = 8, Dc = 1.213 g/cm3, F(000) = 1792, μ(MoKa) = 0.084 mm–1, R = 0.0602 and wR = 0.1445 for 4613 unique reflections with 2272 observed ones (I > 2σ(I)). The results of crystal structure determination show that the title compound has a layer structure, and the two benzene rings in molecule are parallel to each other.
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