Synthesis and Crystal Structure Analysis of 2-(3,5-Di-tert-butyl-2-hydroxyphenyl)-2-(3,4- dimethylphenyl) Acetic Acid Dimethylamine Salt

被引：0
|
作者：
程杰 [1 ,2 ]
成昌梅 [2 ]
何娟 [1 ]
尚培华 [2 ]
王如骥 [2 ]
赵玉芬 [2 ]
机构：
[1] School of Chemistry and Chemical Engineering, Henan University of Technology
[2] Key Laboratory of Bioorganic Phosphorus Chemistry and Chemical Biology, Ministry of Education, Department of Chemistry, School of Life Sciences and Engineering, Tsinghua
来源：
结构化学 | 2009年 / 28卷 / 04期
关键词：
D O I：
暂无
中图分类号：
O621.2 [有机化合物性质];
学科分类号：
摘要：
A new compound 2-(3,5-di-tert-butyl-2-hydroxyphenyl)-2-(3,4-dimethylphenyl) acetic acid dimethylamine salt ([NH2(CH3)2][C24H31O3]) was synthesized and structurally de- termined. It is of monoclinic system, space group P21/c with a = 14.731(2), b = 10.1185(10), c = 17.065(2) , β = 98.293(10)°, Z = 4, V = 2517.0(6) 3, Dc = 1.091 g/cm3, F(000) = 904 and Mr = 413.58. The dihedral angle defined by two benzene rings is 98.23°.
引用
收藏
页码：414 / 418
页数：5
相关论文
共 50 条
  • [1] Synthesis and Crystal Structure Analysis of 2-(3,5-Di-tert-butyl-2-hydroxyphenyl)-2-(3,4- dimethylphenyl) Acetic Acid Dimethylamine Salt
    程杰
    成昌梅
    何娟
    尚培华
    王如骥
    赵玉芬
    Chinese Journal of Structural Chemistry, 2009, 28 (04) : 414 - 418
  • [2] Synthesis and Crystal Structure Analysis of 2-(3,5-Di-tert-butyl-2-hydroxyphenyl)-2-(3,4-dimethylphenyl) Acetic Acid Dimethylamine Salt
    Cheng Jie
    Cheng Chang-Mei
    He Juan
    Shang Pei-Hua
    Wang Ru-Ji
    Zhao Yu-Fen
    CHINESE JOURNAL OF STRUCTURAL CHEMISTRY, 2009, 28 (04) : 414 - 418
  • [3] Behavior of 2-(3,5-di-tert-butyl-2-hydroxyphenyl)benzotriazole (DBHPBT) and 2-(3,5-di-tert-butyl-2-hydroxyphenyl)-5-chlorobenzotriazole during incineration of solid waste contaminated with thousand mg/kg levels of DBHPBT
    Watanabe, Mafumi
    Noma, Yukio
    JOURNAL OF HAZARDOUS MATERIALS, 2010, 178 (1-3) : 1065 - 1069
  • [4] SYNTHESIS AND PROPERTIES OF 2-(3,5-DI-TERT-BUTYL-4-HYDROXYPHENYL)-5-NITROINDAZOLE
    UKHIN, LY
    ORLOVA, GI
    LINDEMAN, SV
    KHRUSTALYOV, VN
    STRUCHKOV, YT
    PROKOFEV, AI
    RUSSIAN CHEMICAL BULLETIN, 1994, 43 (06) : 1034 - 1036
  • [5] Intramolecular interactions of N-(3,5-di-tert-butyl-2-hydroxyphenyl)acetamide derivatives
    M. V. Belkov
    A. N. Harbachova
    G. A. Ksendzova
    G. I. Polozov
    I. V. Skornyakov
    V. L. Sorokin
    G. B. Tolstorozhev
    O. I. Shadyro
    Journal of Applied Spectroscopy, 2010, 77 : 38 - 44
  • [6] Crystal structure of trans-N,N '-bis(3,5-di-tert-butyl-2-hydroxyphenyl)oxamide methanol monosolvate
    Velazquez-Carmona, Miguel-Angel
    Bernes, Sylvain
    Javier Rios-Merino, Francisco
    Reyes Ortega, Yasmi
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2016, 72 : 918 - +
  • [7] INTRAMOLECULAR INTERACTIONS OF N-(3,5-DI-tert-BUTYL-2-HYDROXYPHENYL)ACETAMIDE DERIVATIVES
    Belkov, M. V.
    Harbachova, A. N.
    Ksendzova, G. A.
    Polozov, G. I.
    Skornyakov, I. V.
    Sorokin, V. L.
    Tolstorozhev, G. B.
    Shadyro, O. I.
    JOURNAL OF APPLIED SPECTROSCOPY, 2010, 77 (01) : 38 - 54
  • [8] 2,4-Di-tert-butyl-6-[1-(3,5-di-tert-butyl-2-hydroxyphenyl)ethyl]phenyl 4-methylbenzenesulfonate
    Wu, Jincai
    Pan, Xiaobo
    Wang, Lei
    Yao, Lihui
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2009, 65 : O155 - U2615
  • [9] 2-(3,5-Di-tert-butyl-4-hydroxybenzyl-sulfanyl)nicotinic acid
    Mansor, Shahirah
    Yehye, Wagee A.
    Ariffin, Azhar
    Rahman, Noorsaadah Abdul
    Ng, Seik Weng
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2008, 64 : O1778 - U2132
  • [10] 2-[(3,5-Di-tert-butyl-4-hydroxybenzyl)sulfanyl]benzoic acid
    Alhadi, Abeer A.
    Khaledi, Hamid
    Ali, Hapipah Mohd
    Olmstead, Marilyn M.
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 : O1787 - U436
12345