3,3 '-{[(Biphenyl-2,2 '-diyl)bis(methylene)]bis(oxy)}bis[N-(4-chlorophenyl)benzamide]

被引：0
|
作者：
Rajadurai, Raj [1 ]
Padmanabhan, Ramar [2 ]
Sundaram, Soma Sundaram Meenakshi [1 ]
Ananthan, Sarkkarai [3 ]
机构：
[1] Orchid Chem & Pharmaceut Ltd, R&D Ctr, Chennai 600119, Tamil Nadu, India
[2] Zydus Cadila, Vadodara, India
[3] Presidency Coll, Chennai 600005, Tamil Nadu, India
来源：
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2013年 / 69卷
关键词：
D O I：
10.1107/S160053681301009X
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
In the title compound, C40H30Cl2N2O4, the two benzene rings of the biphenyl unit are twisted with respect to each other, making a dihedral angle of 73.07 (4)degrees. The benzene rings of the benzamide groups form dihedral angles of 77.09 (5) and 55.48 (6)degrees with the central biphenyl moiety. In the crystal, molecules are linked through N - H center dot center dot center dot O hydrogen bonds to form a fused R-2(2)(38) ring motif which forms a supermolecular ribbon network extending along the [100] plane. In the two 4-chlorophenyl rings, the five C atoms and their attached H atoms are disordered over two sets of sites, with site-occupancy factors of 0.657 (15): 0.343 (15) and 0.509 (13): 0.491 (13).
引用
收藏
页码：O914 / +
页数：13
相关论文
共 50 条
  • [1] N,N′-(Biphenyl-2,2′-diyl)bis(furan-2-carboxamide)
    Kee, Chin Hui
    Thomas, Noel F.
    Ariffin, Azhar
    Awang, Khalijah
    Ng, Seik Weng
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2009, 65 : 01556 - U2305
  • [2] N,N′-Bis(3-phenylallylidene)biphenyl-2,2′-diamine
    Dehghanpour, Saeed
    Afshariazar, Farzaneh
    Gao, Shan
    Ng, Seik Weng
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2009, 65 : O307 - U2027
  • [3] N,N′-Bis(4-bromobenzylidene)biphenyl-2,2′-diamine
    Dehghanpour, Saeed
    Asadizadeh, Saeedeh
    Gao, Shan
    Ng, Seik Weng
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2009, 65 : O306 - U2020
  • [4] N,N′-Bis(4-nitrophenyl)biphenyl-2,2′-dicarboxamide
    Wang, Gui-Yu
    Qin, Da-Bin
    Guo, Li-Hui
    Luo, Jie-Wei
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 : O644 - U5263
  • [5] Bis(μ-biphenyl-2,2′-dicarboxylato)bis[(2,2′-bipyridine)copper(II)]
    An, Zhe
    Cui, Rui-Hai
    Zhou, Ru-Jin
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2009, 65 : M412 - U631
  • [6] Bis(μ-biphenyl-2,2′-dicarboxylato)bis[(2,2′-bipyridine)cobalt(II)]
    An, Zhe
    Niu, Xian-Chun
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2008, 64 : M1556 - U710
  • [7] Bis(μ-biphenyl-2,2′-dicarboxylato)-bis[(2,2′-bipyridine)copper(II)]
    Guo, Hong-Xu
    Liang, Min
    Lin, Bin
    Wang, Qing-Hua
    Li, Xi-Zhong
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2008, 64 : M1171 - U632
  • [8] 4,4 '-({[(Pyridine-2,6-diyl)bis(methylene)]bis(oxy)}bis(methylene))dibenzonitrile
    Yamin, Bohari M.
    Kamalulazmy, Nurul A.
    Hassan, Nurul I.
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2014, 70 : 0132 - +
  • [9] 3,3′-Bis(4-chlorophenyl)-2,2′-(m-phenylenedioxy)diquinazolin-4(3H)-one
    Yang, Hai-Zhou
    Gao, Hai-Tao
    Yang, Xu-Hong
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2009, 65 : O59 - U1775
  • [10] N,N′-Bis(2-methoxyphenyl)biphenyl-2,2′-dicarboxamide
    Wang, Gui-Yu
    Li, Di
    Qin, Da-Bin
    Luo, Jie-Wei
    Guo, Li-Hui
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2008, 64 : O2104 - U1812
12345