Determination of diallyl disulfide in garlic by reversed-phase high performance liquid chromatography
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作者:
Wan, Xiaolong
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Inha Univ, Ctr Adv Bioseparat Technol, Nam Ku, 253 Yonghyun Dong, Incheon 402751, South Korea
Inha Univ, Dept Chem Eng, Nam Ku, Incheon 402751, South KoreaInha Univ, Ctr Adv Bioseparat Technol, Nam Ku, 253 Yonghyun Dong, Incheon 402751, South Korea
Wan, Xiaolong
[1
,2
]
Polyakova, Yulia
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Inha Univ, Ctr Adv Bioseparat Technol, Nam Ku, 253 Yonghyun Dong, Incheon 402751, South Korea
Inha Univ, Dept Chem Eng, Nam Ku, Incheon 402751, South KoreaInha Univ, Ctr Adv Bioseparat Technol, Nam Ku, 253 Yonghyun Dong, Incheon 402751, South Korea
Polyakova, Yulia
[1
,2
]
Row, Kyung Ho
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Inha Univ, Ctr Adv Bioseparat Technol, Nam Ku, 253 Yonghyun Dong, Incheon 402751, South Korea
Inha Univ, Dept Chem Eng, Nam Ku, Incheon 402751, South KoreaInha Univ, Ctr Adv Bioseparat Technol, Nam Ku, 253 Yonghyun Dong, Incheon 402751, South Korea
Row, Kyung Ho
[1
,2
]
机构:
[1] Inha Univ, Ctr Adv Bioseparat Technol, Nam Ku, 253 Yonghyun Dong, Incheon 402751, South Korea
[2] Inha Univ, Dept Chem Eng, Nam Ku, Incheon 402751, South Korea
The properties of garlic (Allium sativum L.) are attributed to organosulfur compounds. In this paper, an analytical technique with a rapid and simple sample preparation procedures for determination of diallyl disulfide (DADS) in garlic was reported. The DADS was simply extracted with various solvents (methanol, benzene or tetrahydrofuran) from garlic and prepared for HPLC analysis. From the results, the methanol was select as an optimal extraction solvent. The mobile phase was composed from methanol and water, and the gradient elution mode was applied. 0.61 mg of DADS per g garlic powder can be extracted with methanol. This work offers some advantages over the currently accepted techniques and would be useful for chemical and biological studies of garlic and its products.
机构:
DLO, Rikilt, State Inst Qual Control Agr Prod, NL-6708 PD Wageningen, NetherlandsDLO, Rikilt, State Inst Qual Control Agr Prod, NL-6708 PD Wageningen, Netherlands
Hollman, PCH
Venema, DP
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DLO, Rikilt, State Inst Qual Control Agr Prod, NL-6708 PD Wageningen, NetherlandsDLO, Rikilt, State Inst Qual Control Agr Prod, NL-6708 PD Wageningen, Netherlands
Venema, DP
Khokhar, S
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DLO, Rikilt, State Inst Qual Control Agr Prod, NL-6708 PD Wageningen, NetherlandsDLO, Rikilt, State Inst Qual Control Agr Prod, NL-6708 PD Wageningen, Netherlands
Khokhar, S
Arts, ICW
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DLO, Rikilt, State Inst Qual Control Agr Prod, NL-6708 PD Wageningen, NetherlandsDLO, Rikilt, State Inst Qual Control Agr Prod, NL-6708 PD Wageningen, Netherlands
Arts, ICW
OXIDANTS AND ANTIOXIDANTS, PT A,
1999,
299
: 202
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206
机构:
Sichuan Univ, West China Sch Publ Hlth, Chengdu 610041, Sichuan, Peoples R ChinaSichuan Univ, West China Sch Publ Hlth, Chengdu 610041, Sichuan, Peoples R China
Zou Xiaoli
Li Yuanqian
论文数: 0引用数: 0
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Sichuan Univ, West China Sch Publ Hlth, Chengdu 610041, Sichuan, Peoples R ChinaSichuan Univ, West China Sch Publ Hlth, Chengdu 610041, Sichuan, Peoples R China
Li Yuanqian
Zeng Hongyan
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Sichuan Univ, West China Sch Publ Hlth, Chengdu 610041, Sichuan, Peoples R ChinaSichuan Univ, West China Sch Publ Hlth, Chengdu 610041, Sichuan, Peoples R China
Zeng Hongyan
Zhou Jian
论文数: 0引用数: 0
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Sichuan Univ, West China Sch Publ Hlth, Chengdu 610041, Sichuan, Peoples R ChinaSichuan Univ, West China Sch Publ Hlth, Chengdu 610041, Sichuan, Peoples R China
Zhou Jian
Qin Tingwu
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Sichuan Univ, West China Hosp, Chengdu 610041, Sichuan, Peoples R ChinaSichuan Univ, West China Sch Publ Hlth, Chengdu 610041, Sichuan, Peoples R China
Qin Tingwu
Mo Xiangtao
论文数: 0引用数: 0
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Sichuan Univ, West China Hosp, Chengdu 610041, Sichuan, Peoples R ChinaSichuan Univ, West China Sch Publ Hlth, Chengdu 610041, Sichuan, Peoples R China
机构:
Beijing Hosp Integrated Chinese & Western Med, Dept Clin Lab Med, Beijing, Peoples R ChinaBeijing Hosp Integrated Chinese & Western Med, Dept Clin Lab Med, Beijing, Peoples R China
Zhang, Liang
Yang, Dehui
论文数: 0引用数: 0
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机构:
Shenyang Univ Chem Technol, Dept Chem Engn, Shenyang, Peoples R ChinaBeijing Hosp Integrated Chinese & Western Med, Dept Clin Lab Med, Beijing, Peoples R China
Yang, Dehui
Liu, Ye
论文数: 0引用数: 0
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Capital Med Univ, Obstet & Gynecol Hosp, Beijing Maternal & Child Hlth Care Hosp, Beijing, Peoples R ChinaBeijing Hosp Integrated Chinese & Western Med, Dept Clin Lab Med, Beijing, Peoples R China
机构:
Qingdao Univ, Coll Chem Engn, Qingdao 266071, Peoples R ChinaQingdao Univ, Coll Chem Engn, Qingdao 266071, Peoples R China
Cao Jianmin
Wang Zonghua
论文数: 0引用数: 0
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机构:
Qingdao Univ, Coll Chem Engn, Qingdao 266071, Peoples R ChinaQingdao Univ, Coll Chem Engn, Qingdao 266071, Peoples R China
Wang Zonghua
Ding Mingyu
论文数: 0引用数: 0
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机构:
Tsinghua Univ, Dept Chem, Beijing 100084, Peoples R China
Nanotechnol Industrializat Base China, Tianjin 300457, Peoples R ChinaQingdao Univ, Coll Chem Engn, Qingdao 266071, Peoples R China
Ding Mingyu
Yang Xuedong
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机构:
Tianjin Univ, Coll Pharmaceut & Biotechnol, Tianjin 300072, Peoples R China
Nanotechnol Industrializat Base China, Tianjin 300457, Peoples R ChinaQingdao Univ, Coll Chem Engn, Qingdao 266071, Peoples R China
Yang Xuedong
Kou Huaijiang
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Nanotechnol Industrializat Base China, Tianjin 300457, Peoples R ChinaQingdao Univ, Coll Chem Engn, Qingdao 266071, Peoples R China