1ST-ROW TRANSITION- AND GROUP-12 AND GROUP-14 METAL BIS[HYDRIDOTRIS(3A,7A-BENZO-1,2,3-1H-TRIAZOL-1-YL)BORATE] DERIVATIVES

被引：0
|
作者：
CECCHI, P
LOBBIA, GG
LEONESI, D
PETTINARI, C
SEPE, C
VINCIGUERRA, V
机构：
[1] UNIV CAMERINO,DIPARTIMENTO SCI CHIM,I-62032 CAMERINO,ITALY
[2] UNIV TUSCIA,DIPARTIMENTO AGROBIOL & AGROCHIM,I-01100 VITERBO,ITALY
来源：
GAZZETTA CHIMICA ITALIANA | 1993年 / 123卷 / 10期
关键词：
D O I：
暂无
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
A series of metal complexes analysing as [L](2)M.xH(2)O (0.5 less than or equal to x less than or equal to 2), where L = hydridotris(3a,7a-benzo-1,2,3-1H-triazol-1-yl)borate [(C6H4N3)(3)BH]-; M = Mn, Fe, Co, Ni, Cu, Zn, Cd, Sn, Pb, and V(=O) have been prepared from the appropriate metal chlorides in aqueous solution or CH2Cl2 suspension (Sn and Pb). These compounds were obtained as air-stable solids sparingly soluble in most organic solvents. They have been investigated by elemental analysis, conductivity measurements in DMSO, IR, EIMS spectra and, where possible, H-1 and C-13 NMR spectra. From the collected evidence the compounds are suggested to be polynuclear in the solid state.
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页码：569 / 572
页数：4
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