Preparation and characterization of silica-supported magnetic nanocatalyst and application in the synthesis of 2-amino-4H-chromene-4-carboxylate and 2-amino-5H-pyrano[3,2-c]chromene-4-carboxylate derivatives

被引:0
|
作者
Maleki, Ali [1 ]
Azadegan, Sepide [1 ]
机构
[1] Iran Univ Sci & Technol, Dept Chem, Catalysts & Organ Synth Res Lab, Tehran 1684613114, Iran
关键词
Nanocatalyst; MCRs; Fe3O4; SiO2; Chromene;
D O I
10.3390/ecsoc-19-a017
中图分类号
O62 [有机化学];
学科分类号
070303 ; 081704 ;
摘要
An efficient, one-pot multicomponent procedure for preparation of 2-amino-3-cyano-4H-chromene-4-carboxylate and 2-amino-3-cyano-5H-pyrano[3,2-c]chromene-4-carboxylate using amine-functionalized silica-coated magnetic nanoparticles as a facile prepared, easily recoverable and heterogeneous nanocatalyst was investigated. The catalyst was characterized successfully by Fourier transforms infrared spectroscopy (FT-IR), scanning electron microscopy (SEM) and energy-dispersive X-ray spectroscopy (EDX) analyses. No significant decrease in catalytic activity is another major point of this reusable nanocatalyst.
引用
收藏
页数:5
相关论文
共 50 条
  • [1] Preparation and characterization of silica-supported magnetic nanocatalyst and application in the synthesis of 2-amino-4H-chromene-3-carbonitrile derivatives
    Maleki, Ali
    Azadegan, Sepide
    INORGANIC AND NANO-METAL CHEMISTRY, 2017, 47 (06) : 917 - 924
  • [2] Ethyl 2-amino-5-oxo-4-(p-tolyl)-4H,5H-pyrano[3,2-c]chromene-8-carboxylate
    Wang, J
    Shi, DQ
    Wang, XS
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2004, 60 : O1725 - O1727
  • [3] Ethyl 2-amino-4-(4-methyl-1,3-thiazol-5-yl)-5-oxo-4H,5H-pyrano[3,2-c]chromene-3-carboxylate
    Karthikeyan, V.
    Ramkumar, V.
    Karunakaran, R. Joel
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2013, 69 : O1411 - +
  • [4] Ethyl 2-amino-3-ethoxycarbonyl-7,8-dimethyl-4-[4-(methylsulfanyl)phenyl]-5-oxo-4H-pyrano[3,2-c]chromene-3-carboxylate
    Lakshmi, S.
    Manvar, Dinesh
    Parecha, Alpesh
    Shah, Anamik
    Sridhar, M. A.
    Prasad, J. Shashidhara
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2006, 62 : O2163 - O2165
  • [5] Ethyl 2-amino-4-phenyl-4H-benzo[h]-chromene-3-carboxylate
    Tang, SG
    Gu, XF
    Wei, P
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2006, 62 : O136 - O137
  • [6] Synthesis of 2-amide-3-carboxylate-4-aryl-4H-chromene derivatives
    Zeng, Zhi-gang
    Wang, Lan-ying
    Cao, Yang
    Luo, Yan-ping
    RESEARCH ON CHEMICAL INTERMEDIATES, 2012, 38 (08) : 1751 - 1760
  • [7] Crystal structure of ethyl 2-amino-4-(4-ethoxyphenyl)-5-oxo-4H,5H-pyrano[3,2-c] chromene-3-carboxylate, C23H21NO6
    Liu, Xue-Kun
    Geng, Xiao-Yu
    Zhang, Meng
    Ye, Bai-Jun
    Shi, Zhan
    Wang, Yan-Qiu
    ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES, 2019, 234 (02): : 193 - 194
  • [8] Synthesis of 2-amide-3-carboxylate-4-aryl-4H-chromene derivatives
    Zhi-gang Zeng
    Lan-ying Wang
    Yang Cao
    Yan-ping Luo
    Research on Chemical Intermediates, 2012, 38 : 1751 - 1760
  • [9] Crystal structure of ethyl 2-amino-4-(3-hydroxy-4-methoxyphenyl)-5-oxo-4H,5H-pyrano[3,2-c] chromene-3-carboxylate, C22H19NO7
    Wang, Ning
    Liu, Yu-Hang
    Liu, Da-Wei
    Zhao, Ye
    Wen, Ping
    ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES, 2018, 233 (05): : 813 - 814
  • [10] Crystal structure of ethyl 2-amino-4-(2-methoxyphenyl)-5-oxo-4H,5H-pyrano[3,2-c] chromene-3-carboxylate, C22H19O6
    Wang, Ning
    Liu, Yu-Hang
    Gao, Ming-Lei
    Zhao, Ye
    Wen, Ping
    ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES, 2018, 233 (05): : 807 - 808