PREPARATION AND CHARACTERIZATION OF TRIS(1,10-PHENANTHROLINE) TECHNETIUM(III)

被引：11

作者：

KREMER, C

KREMER, E

机构：

[1] Catedra de Química Inorgánica, Facultad de Química, Montevideo

来源：

JOURNAL OF RADIOANALYTICAL AND NUCLEAR CHEMISTRY-LETTERS | 1993年 / 175卷 / 06期

关键词：

D O I：

10.1007/BF02163748

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

The [Tc(phen)3](PF6)3 complex has been synthesized by ligand substitution on [Tc(tu)6]3+. The reaction proceeds quickly in aqueous solution. A pure compound is obtained with 40% yield. It was characterized by Tc elemental analysis, cerimetric titration, conductometry and electrophoresis. The corresponding spectroscopic properties (UV, Vis, IR and NMR) are also reported and discussed.

引用

页码：445 / 453

页数：9

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