STRUCTURE OF BENZYLTRIPHENYLPHOSPHONIUM IMIDAZOLEBIS(ORTHO-MERCAPTOPHENOLATO)MANGANESE(III) ACETONITRILE SOLVATE

被引：4

作者：

CHEN, XT ^{[1
]}

WENG, LH ^{[1
]}

KANG, BS ^{[1
]}

机构：

[1] CHINESE ACAD SCI,FUJIAN INST RES STRUCT MATTER,FUJIAN 350002,PEOPLES R CHINA

来源：

ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS | 1991年 / 47卷

关键词：

D O I：

10.1107/S0108270191004900

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

C25H22P+.[Mn(C6H4OS)2(C3H4N2)]-.C2H3N, M(r) = 765.82, monoclinic, P2(1)/n, a = 16.221 (4), b = 9.705 (2), c = 24.457 (5) angstrom, beta = 94.96 (1)-degrees, V = 3835 angstrom 3, Z = 4, D(x) = 1.33 g cm-3, lambda(Mo K-alpha) = 0.71073 angstrom, mu = 5.1 cm-1, F(000) = 1592, T = 296 K, final R = 0.054 and wR = 0.064 for 2570 observed reflections with F > 3-sigma(F). The Mn(III) ion is in a distorted square-pyramidal S2O2N coordination environment.

引用

页码：2087 / 2090

页数：4

共 14 条

[1] STRUCTURE OF N,N'-ETHYLENEBIS(SALICYLIDENEIMINATO)MANGANESE(III) CHLORIDE ACETONITRILE SOLVATE
PECORARO, VL
BUTLER, WM
ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 1986, 42 : 1151 - 1154
[2] STRUCTURE OF TRANS-DICHLOROTETRAKIS(THIAZOLE)RH(III) PERCHLORATE . ACETONITRILE SOLVATE
LI, YJ
MA, R
MUIR, MM
MUIR, JA
JOURNAL OF CRYSTALLOGRAPHIC AND SPECTROSCOPIC RESEARCH, 1993, 23 (06): : 493 - 496
[3] STRUCTURE OF TRIS(2-MERCAPTOPYRIDINE 1-OXIDO)COBALT(III) ACETONITRILE SOLVATE
HU, YH
WENG, LH
HUANG, LG
CHEN, XT
WU, DX
KANG, BS
ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 1991, 47 : 2655 - 2656
[4] STRUCTURE OF CHLORO(ALPHA,BETA,GAMMA,DELTA-TETRAPHENYLPORPHINATO)MANGANESE(III) TOLUENE SOLVATE
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FORAN, GJ
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ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 1993, 49 : 236 - 238
[5] STRUCTURE OF BIS(METHANOL)(MESO-TETRAPHENYLPORPHINATO)MANGANESE(III) HEXACHLOROANTIMONATE BIS(TETRACHLOROETHANE) SOLVATE
SCHEIDT, WR
PEARSON, WB
GOSAL, N
ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 1988, 44 : 927 - 929
[6] MIXED-LIGAND COMPLEXES OF TECHNETIUM .12. SYNTHESIS, CHARACTERIZATION AND X-RAY CRYSTAL-STRUCTURE OF (ORTHO-MERCAPTOPHENOLATO)BIS[1,2-BIS(DIMETHYLPHOSPHINO)ETHANE] TECHNETIUM(III) TETRAPHENYLBORANATE, [TC(MEPH)(DMPE)2](BPH4)
MUNZE, R
ABRAM, U
STACH, J
HILLER, W
INORGANICA CHIMICA ACTA, 1991, 186 (02) : 151 - 154
[7] Trichloro(4,4'-dimethyl-2,2'-bipyridine-N,N')- manganese(III) acetonitrile solvate (1/1)
Univ of Florida, Gainesville, United States
Acta Crystallographica, Section C: Crystal Structure Communications, 1998, 54 (pt 2): : 180 - 181
[8] Trichloro(4,4′-dimethyl-2,2′-bipyridine-N,N′)manganese(III) acetonitrile solvate(1/1)
Abboud, KA
Ward, BH
Talham, DR
ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 1998, 54 : 180 - 181
[9] trans-Diaquatetra(nitrato-O,O')dysprosium(III) (18-crown-6)potassium acetonitrile solvate: Synthesis and crystal structure
Chekhlov, A. N.
RUSSIAN JOURNAL OF COORDINATION CHEMISTRY, 2009, 35 (08) : 628 - 631
[10] trans-Diaquatetra(nitrato-O,O′)dysprosium(III) (18-crown-6)potassium acetonitrile solvate: Synthesis and crystal structure
A. N. Chekhlov
Russian Journal of Coordination Chemistry, 2009, 35 : 628 - 631

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