A precursor to highly unsaturated cyclophanes: 7,19,28-trithiatetracylo[11.11.7.1(3,23).1(11,15)]tritriaconta-1,3(32),11(33),12,14,23-hexaene-4,9,16,22,25,30-hexayne

被引：2

作者：

Mague, JT

Ensley, HE

Mahadevan, S

机构：

来源：

ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS | 1995年 / 51卷

关键词：

D O I：

10.1107/S0108270195009073

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

The title compound, C30H18S3.CH2Cl2, has an almost eclipsed conformation with the aromatic rings showing normal van der Waals contacts. The alkyne units in the bridges show some deviation from linearity as a result. The crystal contains solvent dichloromethane which was partially lost in data collection, resulting in a final effective occupancy of 0.55.

引用

页码：2595 / 2598

页数：4

共 7 条

[1] Precursor to highly unsaturated cyclophanes: 7,19,28-Trithiatetracyclo[11.11.7.13,23.111,15]tri -triaconta-1 ,3(32),11(33),12,14,23-hexaene-4,9,16,22,25,30-hexayne
Mague, J.T.
Ensley, H.E.
Mahadevan, S.
Acta Crystallographica, Section C: Crystal Structure Communications, 1995, 51 (pt 12):
[2] 1,3,6,7,9,11,14,15,17,19,22,23,25,27,30,34-HEXADECAAZANONACYCLO[25.5.3.2(6,9).2(14,17).2(22,25).1(3,7).1(11,15).1(19,23).0(30,34)]-TETRATETRACONTANE
DALE, J
ROMMING, C
SUISSA, MR
JOURNAL OF THE CHEMICAL SOCIETY-CHEMICAL COMMUNICATIONS, 1995, (16) : 1633 - 1634
[3] 1,3,7,9,11,15,17,19,23,25,27,34-DODECAAZANONACYCLO[25.5.3.2(6,9).2(14,17).2(22,25)1(3,7).1(11,15).1(19,23).0(30,34)]-TETRATETRACONTANE
DALE, J
ROMMING, C
SUISSA, MR
JOURNAL OF THE CHEMICAL SOCIETY-CHEMICAL COMMUNICATIONS, 1995, (16) : 1631 - 1632
[4] CRYSTAL-STRUCTURE OF 2,8,14,20-TETRAMETHYLPENTACYCLO-[19.3.1.1(3,7).1(9,13).1(15,19)]OCTACOSA-1-(25),3,5,7(28),9,11,13(27),15,17,19(26),21,23-DODECAENE-4,6,10,12,16,18,22,24-OCTOL, C32H32O8
ZAHN, G
SIELER, J
MULLER, K
HENNIG, L
MANN, G
ZEITSCHRIFT FUR KRISTALLOGRAPHIE, 1994, 209 (05): : 468 - 469
[5] Final report on the safety assessment of Ceteareth-2,-3,-4,-5,-6,-7,-8,-9,-10,-11,-12,-13,-14,-15,-16,-17,-18,-20,-22,-23,-24,-25,-27,-28,-29,-30,-33,-34,-40,-50,-55,-60,-80, and-100
Madhaven, BM
INTERNATIONAL JOURNAL OF TOXICOLOGY, 1999, 18 : 41 - 49
[6] CRYSTAL-STRUCTURE OF 2,8,14,20-TETRAMETHYLPENTACYCLO-[19.3.1.1(3,7).1(9,13)1(15,19)]OCTACOSA-1-(25),3,5,7(28),9,11,13(27),15,17,19(26),21,23-DODECAENE-4,6,10,12,16,18,22,24-OCTAETHYL ETHER, C48H64O8
ZAHN, G
MULLER, K
MANN, G
ZEITSCHRIFT FUR KRISTALLOGRAPHIE, 1994, 209 (05): : 473 - 474
[7] The pneumococcal ImmunoArray assay (IAA): Simultaneous detection of IgG responses against 23 pneumocoecal capsular polysaccharide serotypes (1, 2, 3, 4, 5, 6B, 7F, 8, 9N, 9V, 10A, 11A, 12F, 14, 15B, 17F, 18C, 19A, 19F, 20, 22F, 23F, 33F) utilizing a multi-analyte platform.
Lim, L
Lal, N
Patnaik, M
CLINICAL IMMUNOLOGY, 2002, 103 (03) : S132 - S132

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