CHLOROSULFONATION OF 3-METOXYBENZOIC ACID AND ITS METHYL ESTER

被引：0
|
作者：
Agatiev, P. A. [1 ]
Tarasov, A. V. [1 ]
Moskvichev, Yu. A. [1 ]
机构：
[1] Yaroslavl State Tech Univ, Moskovsky Prospect 88, Yaroslavl 150023, Russia
来源：
IZVESTIYA VYSSHIKH UCHEBNYKH ZAVEDENII KHIMIYA I KHIMICHESKAYA TEKHNOLOGIYA | 2013年 / 56卷 / 06期
关键词：
clorosulfonation; 2-sulfobenzoic acid derivatives; anhydride; sulfonamide; saccharine derivatives;
D O I：
暂无
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
It was found that chlorosulfonation of 3-methoxybenzoic acid leads to selective introduction of sulfo group in ortho position with respect to carboxylic group. The ortho-sulfochloride of methyl ester of 3-methoxy benzoic acid was obtained with the subsequent sulfo chlorination of methyl ester of 3-methoxy benzoic acid. This ester is a convenient product for synthesis of 5-methoxy-1,2-benzothiazole-3(2N)-one-1,1-dioxide.
引用
收藏
页码：14 / +
页数：4
相关论文
共 50 条
  • [1] THE PREPARATION OF 2,3,6-TRIHYDROXYBENZOIC ACID AND ITS METHYL ESTER
    KREUCHUNAS, A
    MOSHER, RE
    JOURNAL OF ORGANIC CHEMISTRY, 1956, 21 (05): : 589 - 590
  • [2] Thermodynamic properties of pyruvic acid and its methyl ester
    Emel'yanenko, Vladimir N.
    Turovtsev, Vladimir V.
    Fedina, Yulia A.
    THERMOCHIMICA ACTA, 2018, 665 : 70 - 75
  • [3] NMR characterization of dihydrosterculic acid and its methyl ester
    Knothe, G
    LIPIDS, 2006, 41 (04) : 393 - 396
  • [4] The racemization of an optically active acid and its methyl ester
    Bickel, CL
    JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1938, 60 : 927 - 929
  • [5] ISOLATION OF NATURAL ARACHIDONIC ACID AS ITS METHYL ESTER
    HERB, SF
    RIEMENSCHNEIDER, RW
    DONALDSON, J
    JOURNAL OF THE AMERICAN OIL CHEMISTS SOCIETY, 1951, 28 (02) : 55 - 58
  • [6] Oxidation products of abietic acid and its methyl ester
    Prinz, S
    Müllner, U
    Heilmann, J
    Winkelmann, K
    Sticher, O
    Haslinger, E
    Hüfner, A
    JOURNAL OF NATURAL PRODUCTS, 2002, 65 (11): : 1530 - 1534
  • [7] Electrolytic reduction of abscisic acid methyl ester and its free acid
    Hirai, Nobuhiro
    Iwami, Kumiko
    Horiuchi, Mari
    Kano, Kenji
    Todoroki, Yasushi
    Ohigashi, Hajime
    PHYTOCHEMISTRY, 2012, 80 : 89 - 98
  • [8] INTERACTION OF HYPOPHOSPHORIC ACID AND ITS SALTS WITH DIPHENACYLPHOSPHINIC ACID AND ITS METHYL-ESTER
    FEDOROVA, GK
    ANANEVA, LG
    FESHCHENKO, NG
    ZHURNAL OBSHCHEI KHIMII, 1989, 59 (03): : 717 - 718
  • [9] Oxidation of linoleic acid and methyl linoleate mixed with saturated fatty acid or its methyl ester
    Ishido, E
    Minemoto, Y
    Adachi, S
    Matsuno, R
    LEBENSMITTEL-WISSENSCHAFT UND-TECHNOLOGIE-FOOD SCIENCE AND TECHNOLOGY, 2001, 34 (04): : 234 - 238
  • [10] THERMAL DECOMPOSITION OF METHANCHLOROPHOSPHONIC ACID METHYL ESTER AND METHANCHLOROTHIONOPHOSPHONIC ACID METHYL ESTER
    GRYSZKIE.E
    BULLETIN DE LA SOCIETE CHIMIQUE DE FRANCE, 1967, (06): : 2232 - &
12345