Presentation of sideband envelopes by two-dimensional one-pulse (TOP) spectroscopy

被引：37
|
作者：
Bluemich, B. [1 ]
Bluemler, P. [1 ]
Jansen, J. [1 ]
机构：
[1] Max Planck Inst Polymerforsch, D-6500 Mainz, Germany
来源：
SOLID STATE NUCLEAR MAGNETIC RESONANCE | 1992年 / 1卷 / 02期
关键词：
MAS; 2D NMR; deuteron NMR; quadrupolar nuclei;
D O I：
10.1016/0926-2040(92)90023-3
中图分类号：
O64 [物理化学（理论化学）、化学物理学];
学科分类号：
070304 ; 081704 ;
摘要：
A novel way of representing 1D MAS spinning sideband spectra in a 2D-resolved fashion is explained. The method is illustrated with H-2 MAS data of deuterated polycarbonate. From the resulting 2D spectrum, the istropic shifts can be identified on one axis and the rotary echo decay spectra along the other axis.
引用
收藏
页码：111 / 113
页数：3
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