(E)-3-Methyl-6-(3-oxo-3-(thiophen-2-yl)-1-propenyl)-2(3H)-benzothiazolone

被引：0
|
作者：
Ivanova, Yordanka [1 ]
Gerova, Mariana [2 ]
Chanev, Christo [2 ]
Petrov, Ognyan [2 ]
机构：
[1] Univ Forestry, Fac Ecol & Landscape Architecture, Dept Plant Pathol & Chem, 10 Kliment Ohridsky Blvd, Sofia 1756, Bulgaria
[2] Sofia Univ, Fac Chem & Pharm, Dept Pharmaceut & Appl Organ Chem, 1 James Bourchier Blvd, Sofia 1164, Bulgaria
来源：
MOLBANK | 2016年 / 02期
关键词：
chalcone; 2(3H)-benzothiazolone; thiophene;
D O I：
10.3390/M897
中图分类号：
O62 [有机化学];
学科分类号：
070303 ; 081704 ;
摘要：
The title compound, (E)-3-methyl-6-(3-oxo-3-(thiophen-2-yl)-1-propenyl)-2(3H)-benzothiazolone, was synthesized by Claisen-Schmidt condensation of 3-methyl-2(3H)-benzothiazolone-6-carbaldehyde with 2-acetylthiophene in 94% yield. The structure of the target compound was confirmed using H-1-NMR, C-13-NMR, IR, MS, and elemental analysis.
引用
收藏
页数：3
相关论文
共 50 条
  • [1] (E)-3-Methyl-6-(3-oxo-3-(3,4,5-trimethoxyphenyl)prop-1-en-1-yl)-2(3H)-benzothiazolone
    Ivanova, Yordanka
    Gerova, Mariana
    Chanev, Christo
    Petrov, Ognyan
    MOLBANK, 2016, (03)
  • [2] Studies on the synthesis of 3-methyl-6-(substituted-urea/-thiourea)-2(3H)-benzothiazolone derivatives and antimicrobial activities
    Unal, Ayse Sibel
    Onurdag, Fatma Kaynak
    Ozgen, Selda
    Dogruer, Deniz
    Onkol, Tijen
    INDIAN JOURNAL OF CHEMISTRY SECTION B-ORGANIC CHEMISTRY INCLUDING MEDICINAL CHEMISTRY, 2015, 54 (02): : 253 - 259
  • [3] 3 '-(1H-Indol-3-yl)carbonyl]-1 '-methyl-2-oxo-4 '-(thiophen-2-yl)spiro[indoline-3,2 '-pyrrolidine]-3 '-carbonitrile
    Inglebert, S. Antony
    Arun, Yuvaraj
    Sethusankar, K.
    Perumal, Paramasivam T.
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2013, 69 : O1585 - +
  • [4] Benzyl 2-methyl-3-[(E)-(thiophen-2-yl)methylidene] dithiocarbazate
    Hazari, Saroj K. S.
    Dey, B. K.
    Roy, Tapashi G.
    Ganguly, B.
    Ng, Seik Weng
    Tiekink, Edward R. T.
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 : O1216 - +
  • [5] 1,5-Dimethyl-4-{[(E)-3-oxo-3-(2-thienyl)-1-(trifluoromethyl)-1-propenyl]amino}-2-phenyl-1,2-dihydro-3H-pyrazol-3-one
    Yu, M
    Wang, JL
    Miao, FM
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2002, 58 : O1182 - O1184
  • [6] 4-Hydroxy-6-methyl-3-[3-(thiophen-2-yl)-acryloyl]-2H-pyran-2-one
    Thabti, Salima
    Djedouani, Amel
    Bendaas, Abderrahmen
    Boufas, Sihem
    Loui, Remi
    Mandon, Dominique
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2013, 69 : O524 - +
  • [7] Methyl trans-(+/-)-1-oxo-2-phenethyl-3-(thiophen-2-yl)-1,2,3,4-tetrahydroisoquinoline-4-carboxylate
    Akkurt, Mehmet
    Karaca, Selvi
    Bogdanov, Milen G.
    Kandinska, Meglena I.
    Buyukgungor, Orhan
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2009, 65 : O1287 - U1957
  • [8] N,N-Dimethyl-3-oxo-3-(thiophen-2-yl)propanaminium chloride
    Dayananda, A. S.
    Jasinski, Jerry P.
    Golen, James A.
    Yathirajan, H. S.
    Narayana, B.
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 : O2271 - U2069
  • [9] Crystal structure of 3-{[4-(2-methoxyphenyl)piperazin-1-yl] methyl}-5-(thiophen-2-yl)-1,3,4-oxadiazole-2(3H)-thione
    Al-Alshaikh, Monirah A.
    Abuelizz, Hatem A.
    El-Emam, Ali A.
    Abdelbaky, Mohammed S. M.
    Garcia-Granda, Santiago
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2016, 72 : 269 - +
  • [10] Highly enantioselective bioreduction of N-methyl-3-oxo-3-(thiophen-2-yl) propanamide for the production of (S)-duloxetine
    Tang, Chuan-Gen
    Lin, Hui
    Zhang, Chao
    Liu, Zhang-Qin
    Yang, Tao
    Wu, Zhong-Liu
    BIOTECHNOLOGY LETTERS, 2011, 33 (07) : 1435 - 1440
12345