3-Ethyl-3-hydroxy-8-methoxyquinoline2,4(1H,3H)-dione monohydrate

被引:4
|
作者
Kafka, Stanislav [1 ]
Pevec, Andrej [2 ]
Proisl, Karel [1 ]
Kimmel, Roman [1 ]
Kosmrlj, Janez [2 ]
机构
[1] Tomas Bata Univ Zlin, Fac Technol, Dept Chem, CZ-76272 Zlin, Czech Republic
[2] Univ Ljubljana, Fac Chem & Chem Technol, SL-1000 Ljubljana, Slovenia
关键词
D O I
10.1107/S1600536812043280
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
In the title hydrate, C12H13NO4 center dot H2O, the piperidine ring that is fused to the benzene ring is in a sofa conformation with the chiral C atom lying 0.4084 (18) angstrom out of the plane of the nine fused-ring atoms. In the crystal, O-H center dot center dot center dot O and N-H center dot center dot center dot O hydrogen bonds link the organic molecules and water molecules into chains running along the b-axis direction. The chains are further connected into layers parallel to the bc plane by pi-pi interactions between inversion-related benzene rings [centroid-centroid distance = 3.8846 (9)].
引用
收藏
页码:O3199 / +
页数:9
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