H-1 AND C-13 NMR ASSIGNMENTS OF THE ANTITUMOR MACROLIDE BRYOSTATIN-1

被引：5

作者：

SCHAUFELBERGER, DE

CHMURNY, GN

KOLECK, MP

机构：

[1] Chemical Synthesis and Analysis Laboratory, PRI, DynCorp, National Cancer Institute-Frederick Cancer Research and Development Center, Frederick, Maryland, 21702, P.O. Box B

[2] Sandoz Pharma Ltd, Analytical Research and Development, Basel

来源：

MAGNETIC RESONANCE IN CHEMISTRY | 1991年 / 29卷 / 04期

关键词：

BRYOSTATIN-1; NMR DATA; STRUCTURE;

D O I：

10.1002/mrc.1260290414

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

During a large-scale isolation of bryostatin 1, NMR measurements indicated that parts of the published C-13 and H-1 NMR assignments had to be revised. These reassignments were based on extensive homonuclear and heteronuclear one- and two-dimensional NMR techniques performed at 500 MHz. These independently obtained assignments are also in good agreement with the revised assignments and structure of bryostatin 3.

引用

页码：366 / 374

页数：9

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