SIMPLIFIED METHOD FOR THE DETERMINATION OF ORGANOCHLORINE PESTICIDES IN HONEY

被引：22
|
作者：
MUINO, MAF
LOZANO, JS
机构：
来源：
ANALYST | 1991年 / 116卷 / 03期
关键词：
ORGANOCHLORINE PESTICIDE; HONEY; EXTRACTION; CLEANUP; CAPILLARY GAS CHROMATOGRAPHY;
D O I：
10.1039/an9911600269
中图分类号：
O65 [分析化学];
学科分类号：
070302 ; 081704 ;
摘要：
A method is described for the detection and quantitative determination of organochlorine pesticides in honey. After extraction with hexane, the pesticides were cleaned-up by adsorption chromatography on a Florisil Sep-Pak cartridge and eluted with 15% diethyl ether in hexane. The detection of organochlorine pesticides was performed by capillary gas chromatography with electron-capture detection. The quantification limit obtained for different pesticides ranged from 0.56 to 2.78-mu-g kg-1 and recoveries from fortified honey samples averaged 89.6%.
引用
收藏
页码：269 / 271
页数：3
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