SIMPLIFIED METHOD FOR THE DETERMINATION OF ORGANOCHLORINE PESTICIDES IN HONEY

被引：22
|
作者：
MUINO, MAF
LOZANO, JS
机构：
来源：
ANALYST | 1991年 / 116卷 / 03期
关键词：
ORGANOCHLORINE PESTICIDE; HONEY; EXTRACTION; CLEANUP; CAPILLARY GAS CHROMATOGRAPHY;
D O I：
10.1039/an9911600269
中图分类号：
O65 [分析化学];
学科分类号：
070302 ; 081704 ;
摘要：
A method is described for the detection and quantitative determination of organochlorine pesticides in honey. After extraction with hexane, the pesticides were cleaned-up by adsorption chromatography on a Florisil Sep-Pak cartridge and eluted with 15% diethyl ether in hexane. The detection of organochlorine pesticides was performed by capillary gas chromatography with electron-capture detection. The quantification limit obtained for different pesticides ranged from 0.56 to 2.78-mu-g kg-1 and recoveries from fortified honey samples averaged 89.6%.
引用
收藏
页码：269 / 271
页数：3
相关论文
共 50 条
  • [1] SIMPLIFIED PROCEDURE FOR ORGANOCHLORINE PESTICIDES RESIDUE ANALYSIS IN HONEY
    DRISS, MR
    ZAFZOUF, M
    SABBAH, S
    BOUGUERRA, ML
    [J]. INTERNATIONAL JOURNAL OF ENVIRONMENTAL ANALYTICAL CHEMISTRY, 1994, 57 (01) : 63 - 71
  • [2] Quantitative method for the determination of organochlorine pesticides in serum
    Minelli, EV
    Ribeiro, ML
    [J]. JOURNAL OF ANALYTICAL TOXICOLOGY, 1996, 20 (01) : 23 - 26
  • [3] RAPID METHOD FOR THE DETERMINATION OF ORGANOCHLORINE PESTICIDES IN MILK
    PRAPAMONTOL, T
    STEVENSON, D
    [J]. JOURNAL OF CHROMATOGRAPHY, 1991, 552 (1-2): : 249 - 257
  • [4] A simplified procedure for the determination of organochlorine pesticides and polychlorobiphenyls in edible vegetable oils
    Li, Jindong
    Liu, Donghui
    Wu, Tong
    Zhao, Wenting
    Zhou, Zhiqiang
    Wang, Peng
    [J]. FOOD CHEMISTRY, 2014, 151 : 47 - 52
  • [5] Modification of Method for the Determination of Organochlorine Pesticides in Meat Samples
    Arh, Gregor
    Fras, Simona
    Polak, Tomaz
    Zlender, Bozidar
    Veber, Marjan
    Pompe, Matevz
    [J]. ACTA CHIMICA SLOVENICA, 2009, 56 (04) : 920 - 926
  • [6] ORGANOCHLORINE PESTICIDES IN SEVERAL TYPES OF ROMANIAN HONEY
    Ion, Alina Catrinel
    Ion, Ion
    Culetu, Alina
    [J]. UNIVERSITY POLITEHNICA OF BUCHAREST SCIENTIFIC BULLETIN SERIES B-CHEMISTRY AND MATERIALS SCIENCE, 2011, 73 (03): : 133 - 140
  • [7] Determination of organochlorine and polycyclic aromatic hydrocarbons pesticides in honey from different regions in Romania
    Dobrinas, Simona
    Birghila, Semaghiul
    Coatu, Valentina
    [J]. CHEMICALS AS INTENTIONAL AND ACCIDENTAL GLOBAL ENVIRONMENTAL THREATS, 2006, : 413 - +
  • [8] DETERMINATION OF ORGANOCHLORINE PESTICIDES IN EGG
    SASAKI, K
    SUZUKI, T
    SAITO, Y
    [J]. JOURNAL OF THE FOOD HYGIENIC SOCIETY OF JAPAN, 1988, 29 (03): : 205 - 209
  • [9] DETERMINATION OF ORGANOCHLORINE PESTICIDES IN CHEESE
    BENTABOL, A
    JODRAL, M
    [J]. JOURNAL OF AOAC INTERNATIONAL, 1995, 78 (01) : 94 - 98
  • [10] Small scale method for the determination of selected organochlorine pesticides in soil
    Polese, L
    Minelli, EV
    Jardim, EFG
    Ribeiro, ML
    [J]. FRESENIUS JOURNAL OF ANALYTICAL CHEMISTRY, 1996, 354 (04): : 474 - 476
12345