BREVETOXIN-3 - TOTAL ASSIGNMENT OF THE H-1 AND C-13 NMR-SPECTRA AT THE SUBMICROMOLE LEVEL

被引：16

作者：

CROUCH, RC

MARTIN, GE

DICKEY, RW

BADEN, DG

GAWLEY, RE

REIN, KS

MAZZOLA, EP

机构：

[1] US FDA,GULF COAST SEAFOOD LAB,DAUPHIN ISL,AL 36528

[2] UNIV MIAMI,ROSENSTIEL SCH MARINE & ATMOSPHER SCI,DIV BIOL & LIVING RESOURCES,MIAMI,FL 33101

[3] US FDA,WASHINGTON,DC 20020

来源：

TETRAHEDRON | 1995年 / 51卷 / 31期

关键词：

D O I：

10.1016/0040-4020(95)00360-K

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

The proton and carbon NMR spectra of the marine polyether toxin, brevetoxin-3, are totally assigned using a series of 2D NMR experiments which included: TOCSY, ROESY, HMQC, HMBC, and IDR-(Inverted Direct Response)-HMQC-TOCSY. All work was performed on a sample consisting of 800 mu g (0.95 mu mole) at 500 MHz.

引用

页码：8409 / 8422

页数：14

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