SYNTHESIS AND MOLECULAR-GEOMETRY OF NOVEL DINUCLEAR AND TRI-NUCLEAR IRON COMPLEXES RESULTING FROM INTERACTION OF [FE2(CO)9] WITH R-N=S=N-R(R= TERT-BUTYL OR PARA-TOLYL) - X-RAY CRYSTAL-STRUCTURES OF [FE2(CO)6[RNC(O)S)] AND [FE3(CO)9(RNS)S]

被引：16

作者：

MEIJ, R ^{[1
]}

VANDERHELM, J ^{[1
]}

STUFKENS, DJ ^{[1
]}

VRIEZE, K ^{[1
]}

机构：

[1] UNIV AMSTERDAM,JH VANTHOFF INST,ANORGAN CHEM LAB,AMSTERDAM,NETHERLANDS

来源：

JOURNAL OF THE CHEMICAL SOCIETY-CHEMICAL COMMUNICATIONS | 1978年 / 12期

关键词：

D O I：

10.1039/c39780000506

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

引用

页码：506 / 507

页数：2

共 47 条

[1] CUMULATED DOUBLE-BOND SYSTEMS AS LIGANDS .11. DINUCLEAR AND TRI-NUCLEAR IRON COMPLEXES RESULTING FROM THE REACTION OF [FE2(CO)9]WITH R-N=S=N-R(R=T-C4H9,4-MEC6H4) - CRYSTAL AND MOLECULAR-STRUCTURE OF [FE2(CO)6[RNC(O)S]], [FE3(CO)9(RNS)S] AND [FE3(CO)9(RN)S]
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[2] A NOVEL REACTION BETWEEN [μ-PhC（O）S]-（μ-RS）Fe2（CO）6 AND （μ-R1S）(μ-XMgS)Fe2（CO）6——THE SYNTHESIS, CHARACTERIZATION AND FORMATION MECHANISM OF TWIN CLUSTER COMPLEXES [（μ-RS）Fe2（CO）6]（μ4-S）[（μ-R1S）Fe2（CO）6]
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[3] Synthesis and characterization of double- and triple-butterfly Fe/S cluster complexes obtained from the novel butterfly cluster anions {(μ-RS)(μ-CO)[Fe2(CO)6]2(μ4-S)}- and (μ-RS)(μ-S-)[Fe2(CO)6]3(μ4-S)2.: Crystal structures of (μ-MeS)(μ-PhNHC=S)[Fe2(CO)6]2(μ4-S), (μ-MeS)(μ-MeSC=S)[Fe2(CO)6]2(μ4-S), and (μ-PhCH2S)2[Fe2(CO)6]3(μ4-S)2
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[4] A NOVEL REACTION BETWEEN [MU-PHC(O)S]-(MU-RS)FE2(CO)6 AND (MU-R S-1)(MU-XMGS)FE2(CO)6 - THE SYNTHESIS, CHARACTERIZATION AND FORMATION MECHANISM OF TWIN CLUSTER COMPLEXES [(MU-RS)FE2(CO)6](MU-4-S)[(MU-R S-1)FE2(CO)6]
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[5] Reaction of [Et3NH][(μ-RE)(μ-CO)Fe2(CO)6] (E = S, Se) with azides.: Synthesis of (μ-RE)(μ-p-R1C6H4N3H)Fe2(CO)6 and crystal structure of (μ-ButS)(μ-PhN3H)Fe2(CO)6
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[6] Synthesis of single and double butterfly iron carbonyl complexes by reactions of [(μ-RSe)(μ-CO)Fe2(CO)6]- anions.: Crystal structures of (μ-p-MeC6H4Se)[μ-PhCH2N(H)C=S]Fe2(CO)6 and [(μ-PhSe)(μ-MeAs)Fe2(CO)6]2
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[7] CYCLOPROPENE AS COMPLEX LIGANDS - THE DEVELOPMENT OF A NEW TYPE OF LIGAND BY REACTION OF DIPHENYLCYCLOPROPENTHIONE WITH FE2(CO)9 - THE CRYSTAL-STRUCTURES OF CARBON COMPLEXES WITH AN FE3S2-CLUSTER, C3PH2FE3S2(CO)8, AND A DITHIODIKETONE COMPOUND C6PH4S2FE2(CO)6
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[J]. JOURNAL OF ORGANOMETALLIC CHEMISTRY, 1982, 229 (01) : 63 - 75
[8] CARBONYLIRON COMPLEXES WITH AN AZOMETHYLENE MOIETY .5. PREPARATION OF FE3(PHCH2N)(CO)10 AND HFE3(PHCH=N)(CO)9 FROM BENZALAZINE AND FE3(CO)12 - X-RAY CRYSTAL-STRUCTURE OF MU-(ORTHO-C6H4CH2NN=CHPH)FE2(CO)6
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[J]. JOURNAL OF ORGANOMETALLIC CHEMISTRY, 1986, 302 (02) : 243 - 248
[9] Synthesis and characterization of μ4-S-containing double- and triple-butterfly iron carbonyl complexes.: Crystal structures of (μ-EtS)[μ-PhC(O)S][Fe2(CO)6]3(μ4-S)2 and (μ-t-BuS)2[Fe2(CO)6]3(μ4-S)2
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[J]. INORGANICA CHIMICA ACTA, 2003, 346 : 12 - 18
[10] Synthesis and chemical and electrochemical characterization of Fe-S carbonyl clusters. X-ray crystal structures of [N(PPh(3))(2)](2)[Fe5S2(CO)(14)] and [N(PPh(3))(2)](2) [Fe6S6(CO)(12)]
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[J]. INORGANIC CHEMISTRY, 1996, 35 (04) : 898 - 905

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