A CONVENIENT METHOD FOR THE SYNTHESIS OF O-TERT-BUTYLDIMETHYLSILYL OXIMES

被引：7
|
作者：
ORTIZ, M
CORDERO, JF
PINTO, S
ALVERIO, I
机构：
[1] Department of Chemistry, University of Puerto Rico Humacao
来源：
SYNTHETIC COMMUNICATIONS | 1994年 / 24卷 / 03期
关键词：
D O I：
10.1080/00397919408011200
中图分类号：
O62 [有机化学];
学科分类号：
070303 ; 081704 ;
摘要：
Aromatic, aliphatic, cyclic and acyclic O-tert-butyldimethylsilyl oximes were prepared in 77 to 85% yield by the reaction of the corresponding aldoximes and ketoximes with tert-butyldimethylchlorosilane (TBSCl) using imidazole/DMF system.
引用
收藏
页码：409 / 415
页数：7
相关论文
共 50 条
  • [1] New method for the synthesis of nitriles via the O-tert-butyldimethylsilyl aldoximes
    Ortiz-Marciales, M
    Piñero, L
    Ufret, L
    Algarín, W
    Morales, J
    [J]. SYNTHETIC COMMUNICATIONS, 1998, 28 (15) : 2807 - 2811
  • [2] REDUCTION OF O-TERT-BUTYLDIMETHYLSILYL BENZOLDOXIME
    MORALES, J
    ORTIZ, M
    [J]. ABSTRACTS OF PAPERS OF THE AMERICAN CHEMICAL SOCIETY, 1995, 209 : 276 - CHED
  • [3] The α-alkylation of O-tert-butyldimethylsilyl ketoximes
    Ortiz-Marciales, M
    Quinones, L
    DeJesus, M
    Burgos, C
    Figueroa, D
    Vazquez, L
    Moctezuma, B
    [J]. ABSTRACTS OF PAPERS OF THE AMERICAN CHEMICAL SOCIETY, 1998, 216 : U252 - U252
  • [4] THE REDUCTIVE REARRANGEMENT OF O-TERT-BUTYLDIMETHYLSILYL ARYL OXIMES WITH BORANE.THF COMPLEX
    ORTIZ, M
    SOTO, J
    MORALES, J
    BURGOS, C
    [J]. ABSTRACTS OF PAPERS OF THE AMERICAN CHEMICAL SOCIETY, 1995, 209 : 303 - ORGN
  • [5] Synthesis of silylated O-tert-butyldimethylsilyl aromatic ketoximes.
    Ortiz-Marciales, M
    De Jesús, M
    Morales, EM
    [J]. ABSTRACTS OF PAPERS OF THE AMERICAN CHEMICAL SOCIETY, 2002, 223 : U288 - U289
  • [6] The α-alkylation of aromatic (O-tert-butyldimethylsilyl) ketoximes.
    Ortiz-Marciales, M
    Quinones-Figueroa, L
    Moctezuma, B
    De Jesus, M
    [J]. ABSTRACTS OF PAPERS OF THE AMERICAN CHEMICAL SOCIETY, 1998, 215 : U322 - U322
  • [7] THE REDUCTION OF O-TERT-BUTYLDIMETHYLSILYL KETOXIMES WITH BORANETETRAHYDROFURAN COMPLEX
    ORTIZ, M
    CRUZ, EE
    ALVERIO, I
    [J]. ABSTRACTS OF PAPERS OF THE AMERICAN CHEMICAL SOCIETY, 1993, 206 : 80 - ORGN
  • [8] Efficient α-alkylation and silylation of aromatic O-tert-butyldimethylsilyl ketoximes
    Ortiz-Marciales, M
    De Jesús, M
    Quiñones, L
    Figueroa, D
    Montes, YL
    Burgos, C
    Moctezuma, B
    [J]. TETRAHEDRON, 1999, 55 (42) : 12275 - 12286
  • [9] Synthesis of D-altritol nucleosides with a 3′-O-Tert-butyldimethylsilyl protecting group
    Abramov, M
    Marchand, A
    Calleja-Marchand, A
    Herdewijn, P
    [J]. NUCLEOSIDES NUCLEOTIDES & NUCLEIC ACIDS, 2004, 23 (1-2): : 439 - 455
  • [10] Synthesis of alpha-silylated and alpha-alkylated O-tert-butyldimethylsilyl aromatic ketoximes.
    Ortiz-Marciales, M
    Morales, EM
    De Jesus, M
    [J]. ABSTRACTS OF PAPERS OF THE AMERICAN CHEMICAL SOCIETY, 2003, 225 : U408 - U408
12345