ANTI-2-METHYL-1,3-DITHIANE 1,1,3-TRIOXIDE

被引:2
|
作者
BARKLEY, J
DODD, IM
HARDING, MM
NAMWINDWA, ES
PAGE, PCB
机构
关键词
D O I
10.1107/S0108270192002749
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
C5H10O3S2, M(r) = 182.25, orthorhombic, P2(1)2(1)2(1), a = 9.019 (1), b = 14.522 (1), c = 6.059 (1) angstrom, V = 793.7 angstrom3, Z = 4, D(x) = 1. 525 g cm-3, Mo Kalpha radiation, lambda = 0.71069 angstrom, mu = 5.93 cm-1, F(000) = 384, room temperature, R = 0.031 for 753 reflections with I > 3sigma(I). The S=O bond lengths in -SO2- are 1.426 (3) and 1.432 (3) angstrom while in the -SO- group the S=O bond is substantially longer, 1.497 (3) angstrom.
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页码:2039 / 2040
页数:2
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