LIQUID-CHROMATOGRAPHIC DETERMINATION OF OXYTETRACYCLINE AND CHLORTETRACYCLINE RESIDUES IN ANIMAL-TISSUES

被引：20
|
作者：
HORII, S [1 ]
机构：
[1] TOKYO METROPOLITAN RES LAB PUBL HLTH,SHINJUKU KU,TOKYO 169,JAPAN
来源：
JOURNAL OF LIQUID CHROMATOGRAPHY | 1994年 / 17卷 / 01期
关键词：
D O I：
10.1080/10826079408013446
中图分类号：
Q5 [生物化学];
学科分类号：
071010 ; 081704 ;
摘要：
A simple and sensitive method has been developed for the simultaneous determination of oxytetracycline and chlortetracycline in animal tissues by liquid chromatography(LC). Tissue samples were extracted with EDTA-McIlvaine buffer(ph4.0)/methanol(3/7). The extracts were purified with Sep-pak C18 and Bond Elut SCX cartridges. Two tetracyclines were separated with a synthetic polymer based-ODS column under basic condition. They were determined by LC with programmable fluorometric detector.
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页码：213 / 221
页数：9
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