5-Bromo-4-(3,4-dimethoxyphenyl) thiazol-2-amine

被引：5

作者：

Ghabbour, Hazem A. ^{[1
]}

Chia, Tze Shyang ^{[2
]}

Fun, Hoong-Kun ^{[2
]}

机构：

[1] King Saud Univ, Coll Pharm, Dept Pharmaceut Chem, Riyadh 11451, Saudi Arabia

[2] Univ Sains Malaysia, Sch Phys, Xray Crystallog Unit, George Town 11800, Penang, Malaysia

来源：

ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2012年 / 68卷

关键词：

D O I：

10.1107/S1600536812019320

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

In the title compound, C11H11BrN2O2S, the thiazole ring makes a dihedral angle of 53.16 (11)degrees with the adjacent benzene ring. The two methoxy groups are slightly twisted from the attached benzene ring with C-O-C-C torsion angles of -9.2 (3) and -5.5 (3)degrees. In the crystal, molecules are linked by a pair of N-H center dot center dot center dot N hydrogen bonds into an inversion dimer with an R-2(2)(8) ring motif. The dimers are further connected by N-H center dot center dot center dot O hydrogen bonds into a tape along [(1) over bar 10].

引用

页码：O1631 / +

页数：9

共 50 条

[1] 5-(2-BROMO-4,5-DIMETHOXYPHENYL)-4-(2-HYDROXY-3,4-DIMETHOXYPHENYL)PYRIMIDINE
ARRIETA, JM
DOMINGUEZ, E
LETE, E
VILLA, MJ
GERMAIN, G
VLASSI
ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 1990, 46 : 660 - 663
[2] Total Synthesis of (±)-Joubertinamine from 3-(3,4-dimethoxyphenyl)-5-bromo-2-pyrone
Tam, Nguyen Thanh
Cho, Cheon-Gyu
ORGANIC LETTERS, 2007, 9 (17) : 3391 - 3392
[3] 2-(4-Bromophenyl)-5-(3,4-dimethoxyphenyl)-3,4-dimethylthiophene
Lei, YJ
Shi, JX
Yu, M
Zheng, XF
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2005, 61 : O873 - O874
[4] (E)-1-(2-BROMO-4,5-DIMETHOXYPHENYL)-2-(3,4-DIMETHOXYPHENYL)ETHYLENE
ARRIETA, JM
LETE, E
DOMINGUEZ, E
GERMAIN, G
DECLERCQ, JP
AMIGO, JM
ACTA CRYSTALLOGRAPHICA SECTION B-STRUCTURAL SCIENCE, 1982, 38 (DEC): : 3155 - 3157
[5] (3,4-Dimethoxyphenyl)(4-fluorophenyl)methanone
Lv, Quanjian
Wang, Jianling
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 : O1585 - U694
[6] 2-[4-(benzyloxy)phenyl]-5-(3,4-dimethoxyphenyl)-3,4-dimethylthiophene
Shi, JX
Zheng, XF
Zhu, K
Lei, YJ
Shi, JG
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2004, 60 : O1977 - O1978
[7] 4-tert-Butyl-5-(2,4,5-trimethoxybenzyl)-thiazol-2-amine
Xu, Juan-Juan
Hu, Ai-Xi
Cao, Gao
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2007, 63 : O533 - O534
[8] Transformations of 5-Amino-4-(3,4-dimethoxyphenyl)pyrazoles in the Diazotization Reaction
I. V. Pavlov
K. I. Kobrakov
S. L. Bogza
Chemistry of Heterocyclic Compounds, 2004, 40 (7) : 964 - 965
[9] AN IMPROVED SYNTHESIS OF 5-(3,4-DIMETHOXYPHENYL)-3-HYDROXY-4-NITROCYCLOHEXENE
IBANEZ, AF
MARTINEZ, AR
IGLESIAS, GYM
ORGANIC PREPARATIONS AND PROCEDURES INTERNATIONAL, 1993, 25 (05) : 577 - 606
[10] 4-Bromo-3-{N-[2-(3,4-dimethoxyphenyl)ethyl]-N-methylsulfamoyl}-5-methylbenzoic acid monohydrate
Babu, C. Suneel Manohar
Kavitha, Helen P.
Vennila, Jasmine P.
Chakkaravarthi, G.
Manivannan, V.
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2009, 65 : 01568 - U2415

← 1 2 3 4 5 →